How to make BHO from large amount of trim (5+ lbs)

rolodex ppga

New Member
What would be the best way to prepare BHO from a large volume of trim (5+ lbs)?

I figure there are two ways of going about this...

A) Do a ton of standard butane extractions, using dozens if not hundreds of cans of butane
  • Since there's no extractor big enough to fit so much trim, this would take a lot of time and butane. Is there an appropriate bulk method using tanks of butane? Is there a way to extract 5lb or more in one run?

B) First do a seperate extraction using a different solvent, to get the volume down to something more manageable
  • Then extract that product with butane. I tried this with an ethanol extraction, but the product was too thick and goopy for the butane to seep through it, so there was a very low yield
  • I'm worried about pressure building up and going boom due to butane not being able to seep through... Could this method work better with another type of extract and if so what?

I'd like to hear from the BHO pros... How would you go about this? Thanks for the help!
 

Fadedawg

Well-Known Member
A Mk IA or II Terpenator will extract that volume in about two hours, and a Mk V in about one.

Even a Mk III will process that much material in an afternoon.
 

Sirdabsalot462

Well-Known Member
What FD said..

I suppose you could fashion a custom giant stainless steel tube.

Basically like a giant version of the tube ” Extraction experts. Co....”

My suggestion is similar to your second choice.

Extract bubble first, keep all your quality stuff (45u-73u)..run everything higher, being sure to leave some trim to layer bubble /trim in your tube.
 

Twitch

Well-Known Member
get a big extractor lol guzias has a 5 or 6 foot tube, i just picked up a 3 foot tube it holds over a hp. i have blasted 3lbs with a 1 ounce tube.... needless to say it sucked

and i have packed tubes tight, just make sure that when you pack it, you can still draw air through your extractor effortlessly

find a glass blower
 

Guzias1

Well-Known Member
A Mk IA or II Terpenator will extract that volume in about two hours, and a Mk V in about one.

Even a Mk III will process that much material in an afternoon.
wow.. 5 lbs, in one tube, in 2 hours? wow. and how much butane is needed for he 5 lbs, in a Mk IA or II terpenator?


get a big extractor lol guzias has a 5 or 6 foot tube, i just picked up a 3 foot tube it holds over a hp. i have blasted 3lbs with a 1 ounce tube.... needless to say it sucked

and i have packed tubes tight, just make sure that when you pack it, you can still draw air through your extractor effortlessly

find a glass blower

my big tube can hold anywhere from 2 - 5 ounces depending on my mood.. the fastest i ever blasted 1 lb was in a little over 1 hr..
i could imagine a 2-3 inch wide tube, about 4-5 ft long holding 1 lb or so. i would also imagine three nozzles at one end of the tube to spray 3 cans of butane at once would be nice :]

reclaiming butane sounds even better though.. i really dont understand the terpenators.. butane condenses into a liquid? chilled in a container? then your re-pour? how much is reclaimed? 90-%100 of butane?
 

Twitch

Well-Known Member
wait yours only holds 2 to 5 really??how long is it?

my 1 foot tube holds 80 to 100 grams the one i have now is same diameter but 3 feet long
 

Fadedawg

Well-Known Member
wow.. 5 lbs, in one tube, in 2 hours? wow. and how much butane is needed for he 5 lbs, in a Mk IA or II terpenator?





my big tube can hold anywhere from 2 - 5 ounces depending on my mood.. the fastest i ever blasted 1 lb was in a little over 1 hr..
i could imagine a 2-3 inch wide tube, about 4-5 ft long holding 1 lb or so. i would also imagine three nozzles at one end of the tube to spray 3 cans of butane at once would be nice :]

reclaiming butane sounds even better though.. i really dont understand the terpenators.. butane condenses into a liquid? chilled in a container? then your re-pour? how much is reclaimed? 90-%100 of butane?
A Mk III Terpenator uses about 10 pounds of butane in the system and can reclaim 100%. We typically reclaim 100% of all but the last soak and stop reclaiming it at -22" Hg on the last one, so we lose 25% of the chamber volume in butane vapor, which has a 233:1 ration with liquid butane. The loss is a few pennies.

I've never run longer than a 48" column, and cut back to 36", due to easier loading and unloading.

A Terpenator works by pumping liquid butane through the material in the column, and then evaporating away the butane and recovering it for reuse, using vacuum recovery. Once the butane is recovered, the oil is left behind in the lower chamber.
 

rolodex ppga

New Member
The MK Terpenators look interesting. Would this be the ideal way of going about this? Are they on the market or only homemade? If anybody knows a supplier for them, please PM me.
 

Guzias1

Well-Known Member
You can get plans and open sources for all of their parts at our Skunk Pharm Research site, and Specialized Formulations is selling Mk IIIA kits. They can also get you on a list for one of the other Mk's, which are all custom built.

Here is a picture of an automate Mk II and a Mk III during shakedown.

fade.. with all the new systems coming out.. do you believe this is the route i should pursue ? i am now really interested in the closed system, along with the recovery factor..

i want to put my funds in the right direction though. ive had fun with my 1/4lb borosilicate tube, but the open system, along with the cracked tubes are starting to make me feel like im stuck in progress..

im looking into the MKIII/V systems, along with a cold trap.. do you think im sailing the right way? Opportunities are starting to open up, and your advice would really help me make my investment. i want to produce good oils, nothing less :]
 

Fadedawg

Well-Known Member
fade.. with all the new systems coming out.. do you believe this is the route i should pursue ? i am now really interested in the closed system, along with the recovery factor..

i want to put my funds in the right direction though. ive had fun with my 1/4lb borosilicate tube, but the open system, along with the cracked tubes are starting to make me feel like im stuck in progress..

im looking into the MKIII/V systems, along with a cold trap.. do you think im sailing the right way? Opportunities are starting to open up, and your advice would really help me make my investment. i want to produce good oils, nothing less :]
It would be hard to beat the utility and price of the Mk IIIA, because I designed it as a ma and pa unit that was affordable in kit form.

Last I checked, the Mk IIIA kit was still selling for under $1K from Specialized Formulations, though the component prices from Glacier Tank continue to climb, so ostensibly SF's price will follow. SF passes on the Glacier parts at the same price as Glacier, to keep the price as low as possible, as part of their agreement with us.

The larger units are more oriented towards larger growers or processors and more expensive to build. A lower tank on a Mk IA or II for instance, sells for more that the complete Mk IIIA kit, and an automated Mk V will cost about ten times that much money just to build.

Cost aside, the bigger question may be how much you wish to run at one time. A 24" column on the Mk IIIA holds from about 135 grams to 203 grams, depending on whose packing what, but I pack about 150 grams of prime bud at about 15% moisture content, into that column.

While I designed the Mk IIIA as an affordable ma and pa unit, the larger units are more oriented towards larger growers or processors and more expensive to build. Last I checked, the Mk IIIA kit was still selling for under $1K from Specialized Formulations, though the component prices from Glacier Tank continue to climb, so ostensibly SF's price will follow.

SF passes on the Glacier parts at the same price as Glacier, to keep the price as low as possible, as part of their agreement with us.

A lower tank on a Mk IA or II for instance, sells for more that the complete Mk IIIA kit, and an automated Mk V will cost about ten times that much money just to build.

A Mk IA & II on the other hand, hold up to about 900 grams and a Mk V will hold about 2265 grams under the same packing density.

We've put out that much partially decarboxylated oil for oral consumption in less than a day using a full throttle Mk IIIA. At full throttle in 212F temperature in the hot water pot, the Mk IIIA runs three flood and recover cycles in about 15 minutes, so it can process up to 600 grams per hour

Alas, it runs you to death at that rate, because about the only time you are able to do anything besides watch the gauge and turn valves, is during the final end cycle pump down from when you dump the lower valve, until you hit -22" Hg, and switch to high vacuum.

The product will be also partially decarboxylated, and if your are harvesting carboxylic acid by running a cold pot, it takes about four times as long to cycle, so the output would only be from only 150 grams per hour, to produce light blond shatter of cotton candy consistency.

All of the Terpenators thus far have averaged around 20% yield from the prime bud we extract, and about half that for trim. ~150 grams of bud, has produced about 30 grams of BHO Absolute, and about 8% more measuring the raw oleoresin before winterization, with the plant waxes still present.

All of the larger Terpenators are slower to cycle, but are larger capacity so that you can do something else while it is cycling.

The fully automated versions are the best from a labor standpoint, as they take care of themselves, except for loading and unloading, but it significantly increases the cost to build, because of he need for explosion proof valve operators, all the extra wiring and plumbing, and the electronics themselves. It adds about another $5/10K, depending on how elaborate you want to go.

Our electronics genius is working on an Arduino control package using a pressure transducer, which will be cheaper than the current $840 to build, using a Panasonic controller and pressure switches and should be ready for test soon. Arduino is an open source system for the hobby folks, so I expect lots of bright improvement ideas from the users, once it gets going.
 

Guzias1

Well-Known Member
I really do appreciate the time for your input. I am going to be studying the MKIII terp off skunk farm.. So far, the MKIII seems like the better deal.. A bit more work than a bigger system.. but its efficiency seems pretty nice..

Does Specialized Formations have a website? or do you know what county they are based out of? Having trouble finding them.

Thank you sooooooooooooooooo mucho!
 

Fadedawg

Well-Known Member
I really do appreciate the time for your input. I am going to be studying the MKIII terp off skunk farm.. So far, the MKIII seems like the better deal.. A bit more work than a bigger system.. but its efficiency seems pretty nice..

Does Specialized Formations have a website? or do you know what county they are based out of? Having trouble finding them.

Thank you sooooooooooooooooo mucho!
Portland, Oregon company at http://specializedformulations.com/
 

AlaskaHashMan

Active Member
Got 1.25 pound of sticky trim to run. It's taking forever and is so much work. At the very least I can I'll at least 3 glass tubes...I've run 11 tubes full about 300g and I'm right around 5%.

Obviously getting some cash together and buying a closed system is the way to go, but right now my options are limited.

In over my head?.....
 

Twitch

Well-Known Member
Got 1.25 pound of sticky trim to run. It's taking forever and is so much work. At the very least I can I'll at least 3 glass tubes...I've run 11 tubes full about 300g and I'm right around 5%.

Obviously getting some cash together and buying a closed system is the way to go, but right now my options are limited.

In over my head?.....
get more tubes
 

AlaskaHashMan

Active Member
Indeed, the best place to get them here is in the Valley about an hours drive. Getting a new one tomorrow on the way out of town.
Ran it all finally, just over 33 grams from 584.8. Not to bad, I don't like the deal I have worked out with the grower though. I'm ending up with only half and it's costing me a few hundred in butane.
Need to get a vac purge then my quality will allow me to negotiate the correct deal.
 

Sirdabsalot462

Well-Known Member
Whoa..
33 g's???
Without a vac at all?

Winterize winterize...

You are gonna lose yield but, that's way way too much without having a means of altering atmospheric pressure.

No intentions on sounding dick-ish...
But, we have had some communication, in which you are now a friend of mine.

I do not want a friend dabbing under-purged oil
 

Sirdabsalot462

Well-Known Member
Indeed, the best place to get them here is in the Valley about an hours drive. Getting a new one tomorrow on the way out of town.
Ran it all finally, just over 33 grams from 584.8. Not to bad, I don't like the deal I have worked out with the grower though. I'm ending up with only half and it's costing me a few hundred in butane.
Need to get a vac purge then my quality will allow me to negotiate the correct deal.
Just to elaborate on my above post^...

I started out just like you, hell you are using my tech..lol

But I made small small batches with my toaster oven, when the batches got a little bigger, I purchased a hand vac (25-30$) The brake bleeder
Mity-vac..

I always thought..
” this is pretty good”..why spend more money?

After seeing/performing my first vac session, watching the amount of gas that's trapped within the matrix of the oleoresin.....

My stomach kinda turned, and well, I learned the importance of vacuum purging.

You could also use a sink aspirator as a means of pulling a vac.
Let me know if I can assist any further bro.
 

AlaskaHashMan

Active Member
Scratch that, final weight was 25g.

I'm on it about the vac though maybe getting some help from a member here personally, that's local. I think I may have to get a stainless pressure cooker and get my lexan lid locally. Just don't know about all the plumbing and hoses.

I'll check out a sink aspirator right now.
 
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