Have you used the sous vide method?
I've used oven method for a few batches -- 2 hr @240F. I like the smell but wow, the whole house. Def not stealth. So, I gave sous vide decarboxylation a try based upon this article:
http://marijuanagrowershq.com/decarboxylation-marijuana-alchemy/
In the article linked above, 1 hr 40 minutes at about 200F (93 C)
Sample 3 at 1 hour and 40 minutes was 100% decarboxylated. It appears this would to be a sufficient time and temperature to decarboxylate cannabis with the sous-vide method. Further experiments could reduce this time but batch size, density and starting THC level could also require adjustments. Unless you are going to have your batch lab tested I would not cut down the time or temperature
Also checked kinetics of decarb:
http://cannakb.com/assets/articles/Vaporizer and Other/Decarboxylation of D9thc kenetics and molecular modeling.pdf
Figure 5 in the above link shows 1 hour at 95 C wouldn't be long enough. Plugging numbers into the rate equation confirms that 93 C for 2 hrs should be more than enough time to decarb my weed nearly 100%.
So, that's what I've tried. (Spoiler alert) I get similar or better results using sous vide compared to oven decarb. Based upon my personal response to canna oil made from my home grown.
Some notes on technique:
- Material: small buds from trimming, 1 ounce, "Mastodon" from Oregon Green Seed. Pretty strong smoke, didn't submit for analysis
- Pre-process: scissors to finely chop bud into rice grain-sized bits
- Vacuum packed 1-ounce chopped bud in "boil in bag" with three butter knives for ballast.
Vaccum sealer:
https://www.sorbentsystems.com/sinbosealer.html
- Brought large pot of water to near boil. Checked temperature and submerged bag when pot was "simmer temp", 205 F
- Placed a Japanese "drop lid" to partially cover the surface of the hot water. If fully covered, the water temp would have climbed to nearly 212 and I wanted to keep temp to just below that. An Otoshi-Buta or drop lid can be purchased from Amazon among other places or in a good Asian market.
- Used a digital thermometer to track temperature. Maintained 203 F +/- 5 F
- Total time of treatment: 2 hours
Notes:
- 3 butter knives aren't enough ballast. I had to add external weights and used the drop lid to help keep the package under water.
- Air gained in the package during the treatment. The package was pretty much sucked tightly around the chopped weed but during time, a bubble grew, making it hard to keep the bag submerged.
- The weed got a little damp. Water wasn't leaking through the heat seal. It's my guess that the bag transmits water vapor at near boiling temps. The weed wasn't wet, just a little more moist after processing.
- No odor in the house. Weed smelled good but it did take on some of the tea-like smell that it has when baked in the oven.
Making canna-oil:
- 1 ounce weed to 1 pound coconut oil
- Place weed, oil and water to cover into a pot that fits inside a cheap Presto deep fat fryer. Placed a lid on this pot
- Add enough water to the deep fat fryer to float the small pot. Place a lid on the fat fryer.
- Heat to 190 F, monitor temp closely at first and adjust as needed.
- Stir occasionally
- Once the contents of the inner pot reach 190 F, start timer. Cook for 2 hours. (190 F +/- 5 F for 2 hrs)
- Pour contents into large French press (coffee french press) and push plunger to squeeze out solids.
- Transfer solids from french press to a double sheet of cheese cloth. Squeeze remaining liquid from solid into main batch. Lick fingers.
- Pour off water and oil into a 8x8x2 into glass baking dish. Put into fridge and allow to cool until oil is hard. Place in freezer for a short time if the cake isn't hard enough to lift cleanly off.
- Once oil hardens, lift off from water, discard water.
- Place square oil cake onto cutting board, cut into quarters, package and freeze until needed
Making canna coins:
- Melt 1/4 pound canna oil
- Use silicone candy mold. Mine makes small round flat disks I call "coins".
- 1 tsp per coin.
- Once tray is full, place in freezer several hours until coins freeze solid and hard.
- Pop out coins, place in baggy, put into freezer and enjoy with hot milk.
Result/conclusion:
When I compare oven decarbed canna oil vs the sous vide decarbed canna oil, I find the sous vide coins to be stronger in effect. For me, a lightweight for sure, one coin makes for a pleasant 6 hr buzz. Two coins get me baked. Sous vide coins more so than oven baked but the difference isn't huge.
I'll post more when I learn more. One thing I'll do next time is place twice as much ballast in the bag before vac-sealing it.