.
Katatawnic have you tried making tincture from kief or honey oil? I have a hard time getting the resin to disolve, even in 151 proof rum (still 20% less alcohol per volume than everclear). I let an ounce batch sit since May 31. It's all disolved but I forgot about it until I read your post and he cannaboids have no doubt degraded, not too potent. The taste is much better and you can make the tincture very potent.
What are your thoughts on the speed of dissolving the resin? I want to make glycerin tincture (don't like alcohol) but even heating it I don't get the resin disolved. I've collected the residue from the bottom of a jar, rinsed and strained some in a bubblebag then checked it under a hand microscope and the trichome heads are still round and very much intact. I was thinking of some type of acidic liquid to dissolve the resin, even pouring a touch of liquid butane on it to make honey oil before the resin. I'm impatient and don't have enough extra bud/kief to let things site for 30 or 60 days.
The three things I'm most interested in are potency, speed of preparation, taste - in that order. Any help you could give would be appreciated. Here's the thread where I'm collecting info so you can see where I'm at, all advice is appreciated.
https://www.rollitup.org/cooking-cannabis/125137-alcohol-tincture.html
.
Thanks for sharing your experiences, it's been really helpful. Let me share one of mine with you, should give everyone a laugh and break some tension. My Jar Refining reciepie, similar to what you mentioned, comes with an explosion warning. Perfectly safe though.
.
.
I found a simpler way to refine butter/oil:
Put the cannabutter in a large pyrex mason jar (the more water the better the refinining) and pour in steaming hot water, fill about 3/4. Have a second pyrex container on hand, the same size or larger than the first jar. I use a 2 liter pyrex measuring cup, you could use another mason jar but it must be a wide mouth to get the butter out easily when it hardens.
Put the top on the jar and shake. You'll need oven mitts or a dish town for the heat. Be careful when you shake the jar, the heat from the water will expand the air and if the lid isn't on perfectly tight hot butter will squirt out. Shake up and down easily once or twice to see if the lid is on well. After a couple of shakes it wouldn't be a bad idea to let some of the heated air out of the jar to lower the inside air pressure. Shake for a few minutes to get the chlorophyll, terpins and plant matter (bud & leaf bits, dregs flower, etc).
Pour the mix in the pyrex dish or wide mouth mason jar, or leave in the first jar if it's a wide mouth - less loss. Pour steaming hot water in the first jar, cover and shake to get the rest of the butter that's on the walls, I usually do this twice. Clean your tools (spoons, forks, strainers, etc) with hot water poured over the jar to get butter lost. Pour all this into the wide mouth mason jar.
Into the fridge or freezer to speed cooling and hardening. When the butter hardens into a hard disk cut around the container wall and lift out the butter disk with forks or a spatula. Get the bits of butter out with a spoon or strainer, pour out the foul water, scrape out the rest of the butter. A narrow mouth jar would make removing the butter more difficult.
I found that I lost butter during boiling and on the walls of the pot, and I had to boil out doors because of the smell of boiling Volcano dregs. Absolutely disgusting. I made my last batch of Lava Butter using Dr Jay's Black Out Budd Butter recipe, slow cooker in my grow room so the air filter could take care of the smell - there was hardly any smell except when I stirred the mix. The jar method for refining took care of the rest of the smell.
.
**edit**
Explosion Warning!
I was walking my hounds, thinking about jar refining among other things, when it occurred to me how the shaking of the jar would make 750 ml of water - at 200F+ - contact 250 ml of air - at say an average of 100F. The water would stay about the same temperature but the air would heat up instantly, and try to expand - building pressure.
A rule of thumb for tire pressure is that for every 10 degrees F the temperature changes the tire pressure will change by 1 psi. If we heat the 250 ml (1 cup) of air in the 1 liter jar to 200F we get an increase of 10 psi.
I learned the hard way that even if you think the top is on tight, it may not be. I lost a quarter of my butter on one run, scalding water and boiling fat all over my hands. It took me a second geyser to figure out something was wrong, then a few minutes to think through what I was doing. And that I got off lucky, if the jar had a hairline crack or wasn't a mason jar and the top was tight it could have exploded, scaling more of me with boiling oil and sticking me with with glass shrapnel.
When you have the hot water and butter in the jar put the flat lid on the jar (not the screw on part) and let the air heat up and pop the lid up a few times. It'll let the air inside heat up and the density and pressure won't be as high. It still would be a good idea to shake straight up and down, gently, once or twice and crack the lid to let some of the heated air out.
https://www.rollitup.org/cooking-cannabis/278166-refine-your-cannabuter-better-taste.html
.