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Doesnt matter what solvent u use..ill use hexanes and water n get a pure product free of carcinogens n can get 100% reclamation

Your sox has more poisons then our gas homie...more efficient to use a propane butane mix thank you fadedawg. As fofor gw appreciative of your input im process huge amountbof fan leaf

They got a phone number or website? Propane and butane have differnt recovery temps.?? Would they mix?? Or layer and separate??

Soxhlet is impossible to source in the amount i need..i would also need a stil reclamation setup. Im using gases.

Fractional distillations must be done under vaccum

Water in rotar evap then evap water in purge oven....use ro water

Do you use recovery pumps or passive

Low temps at low humidity.. Darkness...even then like i stated even a stable shatter in perfect settings will begin degradation in 6 months. Acid chains break down. Destabilizes. Butters...

What is the best solvent to run close loop...who is best source to get that solvent... why is it that you went with your choice. I chose propane from bvv

It will always butter even when u learn stability methods..in less kept properly even then shelf life on good shatter is max 6 months

Could be heat aswell maybe not enough...or not a level uneven heat while purging

How long should i let bho sit in spool before opening ball valve

Lipid n fat...winterize before blasting educated blaster have longer life spans

Crucial to distill hexane fully im aware of its carcinogenic property i try not to have any solvent left regardless of it bein more or less poisoning.. Impurity is impurity..im striving to make the cleanest meds using solvents that arent really normal to create... I. E new refinement process

Its very interesting that certain process can be done under just vacuum without heat

Best way of purging hexane??? Vaccum orheat...or both?

What your max negative atmosphere you can acheive with the aspirator??? Brings me to another question could you vacuum purge shatters with a aspirator. Lastly have you done fractional distillation or only simple short path? Thank you any other tips are appreciative.

I guess my real question is where can i get the glassware to do my fractions.. Links would be helpful. Im processing lots. 10L at anytime.

Anyone care to explain any tips to the aspiring bio chemists. Thanks

Reclaim your solvents please! Refine your products leave no solvents. Dont use ridiculous "research" chems. Learn the process from a chemistry site rather then a pot site. Do research before attempts for safety and common sense reasons