Evaporating Green Dragon: Everclear Hash

Fadedawg

Fadedawg

Well-Known Member
Here is a link to our whole QWET procedure. As it is a polar solvent, we don't grind, just break the material up loosely by hand, and we freeze the material and chill the 190 proof to -18C/0F before using a 3 minute soak. http://skunkpharmresearch.com/qwet-extraction/

When the oil is going into an oral, we do a final purge and decarboxylate in a 250F hot oil bath.
 
TheWhiteRabbit420

TheWhiteRabbit420

Active Member
image.jpg

image.jpg


Final product after 24hours of letting the tincture sit out and evaporate.
Hash oil substance, when I made ISO this turned into a glass like ball that melt when burned on top of herb.
 
Muffy

Muffy

Active Member
Fadedawg said:
Here is a link to our whole QWET procedure. As it is a polar solvent, we don't grind, just break the material up loosely by hand, and we freeze the material and chill the 190 proof to -18C/0F before using a 3 minute soak. http://skunkpharmresearch.com/qwet-extraction/ When the oil is going into an oral, we do a final purge and decarboxylate in a 250F hot oil bath.
Click to expand...
So what is it you purge and what "oral" are you talking about, tincture or edibles or some kind?
 
Fadedawg

Fadedawg

Well-Known Member
Muffy said:
So what is it you purge and what "oral" are you talking about, tincture or edibles or some kind?
Click to expand...
In the QWET extraction process, we are purging ethanol. We make more than one oral med and they all are decarboxylated.

The ones I use most myself, are Holy Shit and Holy Anointing Oil Topical. Here are our recipes taken from http://skunkpharmresearch.com/holy-anointing-oil-and-holy-shit/:

Holy Anointing Oil and Holy Shit.

Hi ya’ll, please doooo try this at home because the results are beyond impressive! They are startling.Not only does it provide psychoactive free rapid pain relief used as a topical, but with slight modifications, switch hits sublingually to combine pain relief, with a general uplifting to the spirits and relaxing of the body.

Head effect varies from noticeable in high tolerance patients to blasted in low tolerance patients.Body effect varies from relaxed, to couch locked, depending on tolerance and dosage.

Who knows how old the recipe actually is, because the surviving recipe is from Exodus 30, verses 22-30:22 Then the LORD said to Moses, 23 “Take the following fine spices: 500 shekels of liquid myrrh, half as much (that is, 250 shekels) of fragrant cinnamon, 250 shekels of fragrant cane, 24 500 shekels of cassia – all according to the sanctuary shekel – and a hin of olive oil. 25 Make these into a sacred anointing oil, a fragrant blend, the work of a perfumer. It will be the sacred anointing oil. . . .30 “Anoint Aaron and his sons and consecrate them so they may serve me as priests.

”FirstChurchof the Magi has since risen, who considers the Holy Anointing Oil a sacrament, and more of their thoughts may be found at:http://diversesanctuary.ning.com/page/cann…-holy-anointing.

From the standpoint of process, the perfumers of the time, would have put cinnamon bark, cinnamon leaf, and cannabis bud in olive oil and water. Boiled the water away, strained the oil, and used it in that form.

Eloquentsolution discovered Holy Anointing Oil on another forum pre skunk pharm, and did the math, discovering that the formula called for about 15 ounces of land race cannabis per liter of olive oil, regardless of what else was in it. Whoa!After reading her post on the subject, how could I resist corroborating with making a batch and checking it out?

Since they were using the landrace cannabis of the time, its actual potency is of course conjecture, but there are some clues in the process that they used and the MSDS on cinnamon oil, which says that greater that a 1% solution will burn our skin.Cutting to the chase, we needed essential oils of the additives to maintain continuity of formula, since we were already using essential oils of cannabis. I found the cinnamon bark oil, cinnamon leaf oil, and myrrh gum from http://www.newdirectionsaromatics.com and we have been happy with their service every since.

I made a batch with olive oil, but Eloquentsolution switched her formula from olive oil, to coconut oil, because of coconut oils other salubrious qualities, among them medium chain triglycerides for faster absorption and more rapid passing of the blood brain barrier. Another thought provoking coconut attribute, is that coconut milk is the only natural substance discovered thus far, that can double as blood plasma in humans.

Both of our first batches were impressive, but as Eloquentsolution’s was better, we’ve used coconut oil ever since. She also continued to experiment and developed our current formulas for both Holy Anointing Oil Oral, and Holy Anointing Oil Topical, which have different ratios, and the topical also contains Emu oil. The combination of the cannabis oil and the other ingredients seems to speed up and intensify the results and the whole appears greater than the sum of the parts.

At about the same time, I was also working on my cinnamon Cannapop lollypop recipe, and used a 50% mixture of cannabis oil and Cinnamon candy flavoring oil, fromwww.loranneoils.com.Because the mixture was so tasty, some of the skunk pharmers, who dropped by, started asking for a taste, and asked for it by the name of, “that good shit.”

I therefore named the mix GS, for “Good Shit.”One day I decided to see if Cinnamon candy flavoring oil would ameliorate the slight after taste of HAO sublingual, and when it was successful, I named the mix, “Holy Shit”, or HS.Here are the formulas, both fractionally and in decimals.

Holy Anointing Oil Oral:1 Part Cannabis Oil1/3 Parts virgin unrefined Coconut oil1/15th Part Cinnamon Leaf oil1/15th Part Cinnamon Bark oil1/30th Part liquid Gum MyrrhIE: 1/3 = .3 (.33333333333)1/15 = .07 (.066666666666)1/30 = .03 (.033333333333)

Therefore:

Holy Shit

10 grams BHO Cannabis oil
3 grams Coconut oil
.7 grams Cinnamon Bark oil
.7 grams Cinnamon Leaf oil .
.3 grams Myrrh Gum

Holy Anointing Oil Topical:

10 grams BHO Cannabis oil
8 grams Coconut oil
.7 grams Cinnamon Bark oil
.7 grams Cinnamon Leaf oil .
.7 grams Myrrh Gum1 grams Emu oil* Optional Arnica Montana and/or Jojoba oil

Holy Shit:

10 grams BHO Cannabis oil
3 grams Coconut oil
.7 grams Cinnamon Bark oil
.7 grams Cinnamon Leaf oil .
.3 grams Myrrh Gum
1 gram Cinnamon candy flavoring oil

We make these oils, by adding the other ingredients to the decarboxylated cannabis oil, while the oil is above 82C/180F, and stirring until well mixed. Bottle and use as is.For decarboxylation instructions, check out the tab on our home page, under that name.

Bon appetite!​
 
DemonTrich

DemonTrich

Well-Known Member
this was my 1st attempt at transforming green dragon tincture into green dragon hash (oil), basically my 1st attempt at making anything like this. i hope i did this right. please let me know if i did something wrong, or iif this is dangerous in any way. im a newb at making this kins of stuff.

thanks everyone

i poured remaining green dragon tincture into 9x11 pyrex dish (more evaporating surface area)
filled a roasting pan with 180*/190* water, then put pyrex dish inside it to help in the evap process
once all GDT has evaporated, i scraped all the goodness up and out into a small glass lid
filled a small bowl up with 190* water and placed glass lid in it to melt down the scrapings
5 mins later, all the scrapings melted down uniforminly and is now a nice thick goo (i left it in the bowl for 1/2 hr).

i tried to put a little dab on top of a bowl and smoked it. not sure if that was the proper way to do this, but it was all i have. might have to get a oil vap, but i dont have the spare coin to buy such a rig. but those glass oil rigs most of you all have are freaking insane!!!

pic 1 is just after scraping and put into the glass lid.
pics 2 and 3 are after the 2nd melting


green dragon tincture-oil.jpggreen dragon tincture-oil2.jpggreen dragon tincture-oil3.jpg
 
Fadedawg

Fadedawg

Well-Known Member
Looks good from here!

Better not to combust the oil, both from a flavor, effects, and taste standpoint.

A hot knife and the top cut out of a 2 liter plastic coke bottle for a funnel, is a quick handy vaporization device, if you are short. A borosilicate or quartz wand is usually under $5, and a CP Titanium one under $20.

It is smoother with a water cooling, but you can easily jury rig a water pipe too.

From there a nail or a skillet would be my best suggestion. I use a V-2 KO Domeless Ti Nail, and a HMK swing skillet, both of which work excellently, when you are able to step up a notch. Both were donated for testing, so I don't know the prices, but I just picked up another KO V2 off of a forum for $55, and understand they can be had close to that on line, but no clue on the HMK.

I do know that delivery isn't good with a genuine HMK creation, but worth the wait, or you might check with Aqua Labs for their version.

You can also pick up the generic components for an e-pen that will work, for under $30. Lots of relatively cheap ways to vaporize.
 
DemonTrich

DemonTrich

Well-Known Member
thanks, was hoping i did everything properly.

i went to the local head shop and bought a relatively cheap oil pipe (standard concentrate pipe, no water), a torch and some clean vector butane. im waiting to hear back from my buddy that i got the GDT from, i want to buy him out and make more oil.

heres a pic of the oil/concentrate pipe



oil-concentrate pipe.jpg
 
TheWhiteRabbit420

TheWhiteRabbit420

Active Member
That looks about right demon.
How much did you use and get in return? Did you use shake or nug?

Reheating the oil is a good idea I am going to try this tonight. This would be my 5th run on organic green dragon hash oil.
 
DemonTrich

DemonTrich

Well-Known Member
whiterabbit, i bought the GDT from a buddy of mine. im not sure what he used in making it. i bought a jar of it (12oz ball widemouth jar). it was only filled about 1" max from the bottom. but was enough to fully cover a 9x11" pyrex baking dish. still waiting to hear back from him about buying the rest of his stock. and im about to test out the new oil pipe in a few minutes.


:clap: on the new oil pipe. this oil is pretty damn good. 3 good rips and im good to go.
 
dolamic

dolamic

Well-Known Member
Tincture of cannabis or Green Dragon is an alcoholic solution of Cannabis.

Tincture made from soaking the flowers, leaves, or stems of the Cannabis plant in alcohol. The THC and other Cannabinoids dissolve into the alcohol. Some preparations also extract some of the water-based plant products such as chlorophyll, resulting in a dark green or brown liquid. Baking or "drying" the cannabis to decarboxylate prior to to the alcohol bath increases the potency of the THC in the resulting preparation. Herbs are put in a container and a spirit of 40% or more ethanol is added, 80 proof Vodka or 190 proof Everclear, for example. The jar is left to stand for 2–3 weeks and shaken occasionally in order to maximize extraction. More accurate measuring can be done by combining 1 part herbs with a water-ethanol mixture of 2-10 parts, depending on the herb itself. For most tinctures, however, 1 part water to 5 parts ethanol is typical.

I see nowhere in that about heating the alcohol in an oil bath, or freeze drying anything whatsoever. I am only attempting this, and I'm not trying to degrade someones experience with it, just trying to keep it simple.
I had a bunch of shake and sugar leaves left, ground it up and threw it in a bottle of moonshine. It turned green immediately, and I will see what happens in a couple of weeks. Cheers.
 
TheWhiteRabbit420

TheWhiteRabbit420

Active Member
Right.. ^^

This thread is about making HASH OIL. I think we all know how to make Green Dragon...Soak the herb in alcohol. Done...

Now when it comes to making Quality, Organic Hash Oil FROM Green Dragon that is where the following information comes in..

Freezing the marijuana prior to making the solution helps with the extraction. The trichomes freeze and separate from the plant material much quicker.
I've made about a dozen extractions this way and the result is pretty consistent.
Heating the alcohol is what people do if they want to speed up the proccess. Again...Has NOTHING to do with making Green Dragon.. But has everything to do with Hash which is what this thread is about..
When EVAPORATING the tincture you are left with a Hash oil. This takes at least 24 hours depending on the amount of herb you're using.. I made some Hash using a half pound of herb and this took 4 days to evaporate.
By boiling off or heating up the alcohol to it's boiling point you are letting the solvent evaporate to leave you with Hash Oil.


:D
 
TheWhiteRabbit420

TheWhiteRabbit420

Active Member
Guzias1 said:
where do you rec i buy some damn Everclear? i did some shopping around here in the local area of nor cal. aint got none dat!
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Unfortunately 190proof alcohol is illegal in a handful of states Cali being one of them. I'm not sure if youcan find anything close enough. Bacardi 151 might work but I've never tried it.
 
I

ilikecheetoes

Well-Known Member
i get my everclear from winechateau.com spelling might not be right there... they ship to cali.

so wait since you need to decarb to get effect from eating canna. whats the point of green dragon?
 
M

MedicalMan702

Member
SnakeByte said:
DO NOT CONSUME ISO HASH. Isopropyl Alcohol is created chemically and is meant as fuel addative and for external use ONLY. It won't kill you instantly but not good for you like Naphtha hash.
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Isn't all the naphtha or iso alcohol evaporated out from the boiling? Rick Simpson in Run from the Cure uses naphtha and suggests it in his recipe for making THC oil.
 
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