rob333
Well-Known Member
lol stay away from the stuff under the kitchen sink bro
Making LSD/PCP - Is this a joke?
- Thread starter Karmapuff
- Start date
Frigyes layman
New Member
Ok it seems I was wrong and can admit it here is the actual and very simple recipe for 4-MeO-Phencyclidine Now all instructions can be found on Erowid but here it is
A solution of 6.3g sodium bisulfite in 21 mL of water was cooled in an ice bath. 5.3g (5.03 mL) of cyclohexanone was added with rapid stirring. This resulted in a thick white slurry. A solution of 3.93g if potassium cyanide in 9.48g (8.17 mL of piperidine was added to the slurry. The slurry turned into a two-phase reaction mixture, which was allowed to stir overnight. The next morning, stirring was stopped, and the mixture was cooled on ice. The upper oily phase soon crystallized as beautiful ice-like crystals. These were removed by filtration, washed well with cool water, and dried between paper towels.
1.9g (.08 moles) of Magnesium turnings were placed in a round bottom flask, along with a magnetic stirbar and 30 mL of dry ether. In a second flask, a solution of 15.2g (0.08 mol.) of 4-methoxy bromobenzene (i.e. 4-bromo anisole, see Note 1) in 10 mL of ether was prepared. Approximately 9 mL of the bromobenzene solution was added to the flask containing the ether/magnesium. This flask was then gently heated and stirred until the reaction began, as indicated by formation of a cloudy gray precipitate. The remaining ether/bromobenzene solution was added at a rate that allowed for gentle reflux (see Note 2 and Note 3).
A solution of 3.5g (0.02 mol) of the compound from step 1 was dissolved in a small amount of toluene (~10 mL). This solution was then dried over calcium chloride, filtered, and then diluted with an equal amount of anhydrous ether. This was slowly added to the Grignard reagent prepared in step 2, followed by heating and stirring for 2 hours. The reaction mixture was then poured onto a mixture of several grams of ammonium chloride and ice, with stirring. After bubbling stopped, several grams of sodium hydroxide was added and the mixture was shaken in a seperatory funnel. The lower aqueous phase was separated, shaken with fresh ether, and discarded. The combined organic phases were washed 3 times with water, and the water layers discarded. The organic layer was then extracted 3 times with dilute hydrochloric acid. The acid layers were basified with sodium hydroxide and then extracted with ether. The combined ether layers were evaporated to give ~2.5g of a colorless oil (see Note 4). After sitting for 2 days, followed by cooling in a freezer, the oil began to crystallize into awesome colorless crystals.
A solution of 6.3g sodium bisulfite in 21 mL of water was cooled in an ice bath. 5.3g (5.03 mL) of cyclohexanone was added with rapid stirring. This resulted in a thick white slurry. A solution of 3.93g if potassium cyanide in 9.48g (8.17 mL of piperidine was added to the slurry. The slurry turned into a two-phase reaction mixture, which was allowed to stir overnight. The next morning, stirring was stopped, and the mixture was cooled on ice. The upper oily phase soon crystallized as beautiful ice-like crystals. These were removed by filtration, washed well with cool water, and dried between paper towels.
1.9g (.08 moles) of Magnesium turnings were placed in a round bottom flask, along with a magnetic stirbar and 30 mL of dry ether. In a second flask, a solution of 15.2g (0.08 mol.) of 4-methoxy bromobenzene (i.e. 4-bromo anisole, see Note 1) in 10 mL of ether was prepared. Approximately 9 mL of the bromobenzene solution was added to the flask containing the ether/magnesium. This flask was then gently heated and stirred until the reaction began, as indicated by formation of a cloudy gray precipitate. The remaining ether/bromobenzene solution was added at a rate that allowed for gentle reflux (see Note 2 and Note 3).
A solution of 3.5g (0.02 mol) of the compound from step 1 was dissolved in a small amount of toluene (~10 mL). This solution was then dried over calcium chloride, filtered, and then diluted with an equal amount of anhydrous ether. This was slowly added to the Grignard reagent prepared in step 2, followed by heating and stirring for 2 hours. The reaction mixture was then poured onto a mixture of several grams of ammonium chloride and ice, with stirring. After bubbling stopped, several grams of sodium hydroxide was added and the mixture was shaken in a seperatory funnel. The lower aqueous phase was separated, shaken with fresh ether, and discarded. The combined organic phases were washed 3 times with water, and the water layers discarded. The organic layer was then extracted 3 times with dilute hydrochloric acid. The acid layers were basified with sodium hydroxide and then extracted with ether. The combined ether layers were evaporated to give ~2.5g of a colorless oil (see Note 4). After sitting for 2 days, followed by cooling in a freezer, the oil began to crystallize into awesome colorless crystals.