Proper & Pure n,n-DMT pull / extraction

QUAD BREATH

Well-Known Member

• Jun 27, 2019

• #21

HeatlessBBQ said:

It looks a bit like the lower layer of the Extraction Mixture; once extracted / evaporated.

Click to expand...

HeatlessBBQ said:

Wonder how and what the effects are like with Lime tek...?

Click to expand...

I don't think it is a lower layer as there isn't a lower layer in this tek. Further, the naphtha is perfectly clear when decanted to pyrex dish.

Anyways, here is some really good information on Jungle Spice and other alkaloids:
https://wiki.dmt-nexus.me/w/images/b/b7/Jungle_Spice.pdf

Usually, if you want a full spectrum product you use something like xylene as indicated in Q21's tek. In fact, after you pull your pure white DMT you can go back with xylene and extract the other alkaloids.

I was a little puzzled because I was just using naphtha. However, with Q21's tek two-thirds of the naphtha would soak into the bark and would remain in there (and evaporate too) until next pull. Perhaps, the build up of naphtha and evaporation caused some sort of reaction ...not sure. I do know one thing, it smells just like DMT - that is why I believe this is some form of Jungle or Jimjam.

I should further note, SWIM is in Canada and is using Ronsonol lighter fluid and the formula changed in 2010 (?) when Zippo bought them out. The CAS #'s are 68410-97-9 and #6472-49-0. It is also worth noting that an evaporation test was done on this fluid and it left NO residuals.

 

Last edited: Jun 27, 2019

HeatlessBBQ

Well-Known Member

• Jun 27, 2019

• #22

Preparing Your RB Mixture:

Step 2.) Add Water. 500 mL [into an open, tempered glass container]








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HeatlessBBQ

Well-Known Member

• Jun 27, 2019

• #23

Step 3.) Add Sodium Hydroxide. About 200 mL ~ Mix / Wait






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HeatlessBBQ

Well-Known Member

• Jun 27, 2019

• #24

Step 3-B.) Let Mixture settle.





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HeatlessBBQ

Well-Known Member

• Jun 27, 2019

• #25

Step 4.) Add RB. 50-100 grams

~ Mix / Wait






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Last edited: Jun 27, 2019

HeatlessBBQ

Well-Known Member

• Jun 27, 2019

• #26

Step 4-B.) Let Mixture settle.






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Last edited: Jun 27, 2019

WildCard008

Well-Known Member

• Jun 27, 2019

• #27

hey man bbq you are fucking crazy

 

HeatlessBBQ

Well-Known Member

• Jun 28, 2019

• #28

The Extraction:


Step 6.) Mix / Heat / Wait x3-7.

[boil a pan of water, take off, set glass container containing mixture in hot water]






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Last edited: Jun 28, 2019

HeatlessBBQ

Well-Known Member

• Jun 28, 2019

• #29

Step 7.) Add Naphtha to Mixture.

[before this step you can divide glass container x2-3 - optional]






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HeatlessBBQ

Well-Known Member

• Jun 28, 2019

• #30

Step 8.) Mix / Heat / Wait x3-7. [keep glass container/s open & not sealed]

[boil a pan of water, take off to OUTSIDE, set glass container/s containing mixture in hot water]






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HeatlessBBQ

Well-Known Member

• Jun 28, 2019

• #31

Step 8-B.) Let Mixture Settle






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Purpsmagurps

Well-Known Member

• Jun 28, 2019

• #32

nice job! I hear going straight to base cyb tech is the way to go, not removing fats before going polar.

 

HeatlessBBQ

Well-Known Member

• Jun 28, 2019

• #33

The Extraction [Part 2]:


Step 9.) Let Mixture settle into TWO layers [Naphtha on top. Sodium Hydroxide/RB on bottom].

[The top layer should have dissolved / emulsified the n,n-DMT into the naphtha.]


Step 10.) Decant the top layer into a glass container/s. DO NOT decant any bottom layer!!!






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Last edited: Jun 28, 2019

HeatlessBBQ

Well-Known Member

• Jun 28, 2019

• #34

Step 11.) Collect the Naphtha that contains the DMT into a separate glass container/s to Precipitate.


Step 12.) Repeat steps 7-10 {two, three or more times for a better yield}. [optional]

[2 extra glass containers may be needed]






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HeatlessBBQ

Well-Known Member

• Jun 29, 2019

• #35

Step 13.) Let Naphtha containing DMT settle. [crystals start forming]



[STEP 12 repeat optional IF NEEDED-not that hard]






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HeatlessBBQ

Well-Known Member

• Jun 29, 2019

• #36

Purpsmagurps said:

nice job! I hear going straight to base cyb tech is the way to go, not removing fats before going polar.

Click to expand...

Removing the base layer does seem to a be a much better alternative.

New Holiday gift wish list perhaps?

 

Purpsmagurps

Well-Known Member

• Jun 29, 2019

• #37

I love that jungle. hits harder stays longer. less hyperactivity and you can actually pay attention to your blast off. I hit it pretty hard on the dab nail.

 

Purpsmagurps

Well-Known Member

• Jun 29, 2019

• #38

n-oxide then zinc and acetic, turns to freebase, you do that? my friend is a chemist and does this on the side of his extraction biz.

 

HeatlessBBQ

Well-Known Member

• Jun 29, 2019

• #39

Purpsmagurps said:

I love that jungle. hits harder stays longer. less hyperactivity and you can actually pay attention to your blast off. I hit it pretty hard on the dab nail.

Click to expand...

I don't know about that one, Mate.
You may be more right than I.

Some are weary towards that jimjam, man... IT could however, be...a rumor.
But the intuitive forces are strictly forbidding IT's availability to SWIM and eYE.

Purpsmagurps said:

n-oxide then zinc and acetic, turns to freebase, you do that? my friend is a chemist and does this on the side of his extraction biz.

Click to expand...

Pretty sure SWIM didn't go that way... Processing...
SWIM has sent in His PMs.

Taking an Acetic wash. What about K hydroxide?

 

Last edited: Jun 29, 2019

Purpsmagurps

Well-Known Member

• Jun 29, 2019

• #40

STB in a pressure cooker actually , with solvent, straight to base, , then you have your oxides which is a LOT OF WEIGHT!!! , the oxide bring the oils into the final product increasing your yield and in my opinion gives you a GREAT experience, full spectrum, you can re-ex the end and it might be less steps idk but my guy swears by it and he says his yields are great.

 

Last edited: Jun 29, 2019