Twitch
Well-Known Member
back then I would run the temps at 130 to 135 degrees Fahrenheit and I would let the vacuum pump run continuously anywhere from 4 to 36 hours sometimes longerWhat's your cook Temps and times
back then I would run the temps at 130 to 135 degrees Fahrenheit and I would let the vacuum pump run continuously anywhere from 4 to 36 hours sometimes longerWhat's your cook Temps and times
Would pump at -26 work that's the best vac I can getback then I would run the temps at 130 to 135 degrees Fahrenheit and I would let the vacuum pump run continuously anywhere from 4 to 36 hours sometimes longer
I don't loose many terps because i can keep my temps low during vacuum distillation. Thats a closed loop absolute etoh extraction so i reclaim or "purge" at a range of about 6 to 12 degrees.got to say that is most impressive there gw. What was the terpene retention like, or was it not so good prior to cleaning?
So what polar solvent do you use? And how do you selectively wash chlorophyll? Super salinated solution?I don't loose many terps because i can keep my temps low during vacuum distillation. Thats a closed loop absolute etoh extraction so i reclaim or "purge" at a range of about 6 to 12 degrees.
After the solvent is gone, temps rise on their own to the next bp's from 30 to 60. I let it do this to thicken the oil and boil off some of the nasties.
The whole reclaim/purge process takes about 5 hours yeilding about a half pound of thc oil. I suppose if you wanted to call it shatter you could spread it out thin layer and put it in a vacuum drying oven. But it would only take about 2 hours at 60 degrees. And i give you "shatter". Not 5 days like bho.
My cleaning process is to remove the chlorophyll that comes from a polar extract. That takes minutes.
As compared to supercritical wax derivative oil extraction i get higher yeilds and do it all from trim to finished oil in 24 hours and use nothing poisonous.
I process 500 grams of trim per run yeilding 200 to 250 thc oil with terps. over 85% delta 9
Dont mean to brag but i like to anyways.
Hopefully it inspires someone to look elsewhere for extraction methods.
This looks like the 'red oil' that Raphael mechoulam made in the 60s? Which was the best attempt at the time at pure the.[/QUOTE
I got time to hear about chlorophyll, and I was under the impression that pharmeceutical patents could not be renewed and had a statute. 76 years is a long time for any patent...Etoh
Chlorophyll is a long story.
Funny you should mention Raphael because it seems like only people that were around in the 50's and 60's remember that cannabis oils are red.
We both use(d) a method similar to one that was patented in 1940 by a major pharmaceutical company and the patent is still maintained today.
This attitude is what I hate the most about the cannabis industry, the lack of trust and reciprocation. Btw I found a modern patented process for both purifying cannabinoids and acetylizing them. In 5 minutes on google patents. So how dumb do you think I and everyone else is? I've had to sign NDA's just growing up in the town I did and I'm done with it. Share the love, there is little going around these days.Another long story. (Patents) probably not the propper place for such specific topics like patent law and chlophyll.if you have any questions pm me
or research on your own,
anywhere but google and definitely not in online discussion forum. The truth is out there you just have to peal away the layers of garbage (google)
I was just suggesting that we were perhaps thread jacking a sticky and maybe the conversation should be moved elsewhere or you should research on your own which is what you did and exactly what I wanted you to do haha. Once you gain the knowledge you seek is start executing it I guarantee you will feel differently about sharing so freely what you worked so hard to attainThis attitude is what I hate the most about the cannabis industry, the lack of trust and reciprocation. Btw I found a modern patented process for both purifying cannabinoids and acetylizing them. In 5 minutes on google patents. So how dumb do you think I and everyone else is? I've had to sign NDA's just growing up in the town I did and I'm done with it. Share the love, there is little going around these days.